File:NDL1045501 大阪工業試験所報告 第19回 第9号 チタン顔料の研究第1報.pdf

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大阪工業試験所報告   (Wikidata search (Cirrus search) Wikidata query (SPARQL)  Create new Wikidata item based on this file)
Author
大阪工業試験所 (商工省)
image of artwork listed in title parameter on this page
Title
大阪工業試験所報告
Volume 第19回 第9号 チタン顔料の研究第1報
Publisher
工業調査協会
Language jpn
Publication date

1942

昭和13-17
Place of publication JP
Source

doi:10.11501/1045501

institution QS:P195,Q477675
Creator
InfoField
商工省大阪工業試験所 編
Publication Place
InfoField
東京
Subject: NDC
InfoField
504
Extent
InfoField
22冊 ; 26-27cm
Material Type
InfoField
Book
Source Identifier: JPNO
InfoField
46035383
Date Digitized: W3CDTF
InfoField
2010-03-31
Audience
InfoField
一般
Title Transcription
InfoField
オオサカ コウギョウ シケンジョ ホウコク
Volume Transcription
InfoField
00090
Publisher Transcription
InfoField
コウギョウ チョウサ キョウカイ
Source Identifier: NDLBibID
InfoField
000000696320
Call Number
InfoField
14.2イ-498
Creator: NDLNAId
InfoField
00266723
Type: summaryPartition
InfoField
1
Contents
InfoField
標題

目次

第一章 緒言/1

第二章 チタン顏料の製造法に關する從來の研究/2

1. 鹽素法/2

2. 熔融法/3

3. 硫酸法/3

4. 還元法/4

5. 窒化法/4

6. 弗化水素法及其他の方法/5

第三章 硫酸法による酸化チタンの製造法の研究/5

(I) 鑛石/5

(II) 鑛石と硫酸との反應/6

1. 實驗方法/6

2. 分析方法/6

3. 抽出に使用する水の量/8

4. 攪拌と鑛石の溶解率/9

鑛石の分解率の計算方法/11

5. 鑛石の粒の大さと鑛石の溶解率/12

6. 硫酸の濃度と鑛石の溶解率/14

7. 加熱慍度と鑛石の溶解率/15

8. 硫酸の量と鑛石の溶解率/19

(III) 鑛石の硫酸溶液の處理/19

1. H2SO4‐FeSO4‐H2O系の0℃における平衡/23

2. 鐵の硫酸溶液中の遊離硫酸の定量法/30

3. 遊離硫酸の計算方法/31

4. 冷却に依る鐵分の除去/32

5. 濃縮液の冷却、晶出/34

(IV) 硫酸チタン溶液の加水分解/36

1. 遊離硫酸の定量法/38

2. 豫備實驗/38

3. 液中の遊離硫酸の量と加水分解率/39

A. 1.6gTiO2/l溶液/39

B. 0.6gTiO2/l溶液/40

4. チタン溶液の濃度と加水分解率/41

5. 加熱慍度と加水分解率/42

6. 加熱時間と加水分解率/43

7. 遊離硫酸と酸化チタンとの量の比と加水分解率/45

A. 遊離硫酸/酸化チタン=0.5の場合/46

B. 遊離硫酸/酸化チタン=1の場合/46

C. 遊離硫酸/酸化チタン=2の場合/47

D. 遊離硫酸/酸化チタン=3の場合/47

E. 遊離硫酸/酸化チタン=4の場合/49

F. A~Eの總括/49

G. 加熱時間と加水分解率/50

8. 添加鹽類と加水分解率/51

A. 種々の鹽類の凝集力の比較/51

B. 添加鹽類と加水分解率/53

C. 添加鹽類の量/54

9. 加水分解の條件と酸化チタンの粒子の大きさ/57

A. 遊離酸の量と粒子の大きさ/57

B. 加水分解時間と粒子の大きさ/58

C. 添加食鹽の量と粒子の大きさ/63

10. 鐵分多き溶液の加水分解/64

11. 其他の條件と加水分解率/69

12. 高慍度における加水分解/70

A. 慍度の影響/71

B. 加熱時間の影響/73

C. 還元程度の影響/74

D. TiO2の濃度の影響/75

(V) 沈澱の濾過及洗滌/77

1. 洗滌液の種類/77

2. 洗滌回數/81

(VI) 沈澱の焙燒/83

1. 焙燒慍度/83

A. 焙燒慍度とTiO2の色相/83

B. 焙燒慍度と比重/85

C. 焙燒慍度とTiO2の吸油量、被覆力、着色力及び其他の性質/86

2. 焙燒時間/89

A. 焙燒時間とTiO2の色相/89

B. 焙燒時間と比重/89

3. 添加鹽類の影響/90

(VII) 製品の諸性質とその改良/91

1. 琺瑯施釉試驗/91

2. グリセリン變色試驗/99

3. 製品中の不純物/100

A. 鐵分の比色定量/100

B. 硫酸に溶けざる部分/100

4. 比重/102

5. 被覆力/105

6. 吸油量/105

7. 着色力/105

8. ペイント耐候試驗/106

A. 日光曝露試驗/106

B. 紫外線曝露試驗/109

9. 粒子の大きさ/120

(VIII) 工業化に關する諸問題/127

1. 機械裝置及びその材料/127

2. 副産物及び廢液處理/129

3. 1ton規模の設備費及び生産費概算/129

第四章 還元法による酸化チタンの製造法の研究/130

1. 實驗方法/131

2. 豫備實驗/132

3. 還元慍度/133

4. 酸化焙燒の影響/136

5. 觸媒の影響/137

6. 酸化焙燒鑛石に對する觸媒の影響/139

7. 總括/140

第五章 要旨/140

文献/142

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